METX Test Results




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METX Engine Formula



Testing Procedures & Results 
METX has subjected its products to a number of tests (with no modification) performed by third party, world renowned, industry accepted and respected laboratories.  Those tests include, but are not limited to the following: 

(A)   METX Engine Formula: 

ASTM D testing of the product through the use of the Block-on-Ring Tester and the Seta Shell Four Ball Test machine (ASTM D-2509, D-4172 and D-2782), Pin & Vee Block (ASTM D-2670, D-2625 and D-3233) demonstrates the ability of the product to perform as an extreme pressure additive.

Each of these test machines incorporates a rotating steel surface applied against a fixed steel surface while submerged in a bath of the test lubricant.  Pressure is noted as kilogram force (KGF) applied to the mating surface while the rotating surface is set for a fixed RPM (revolution per minutes). 

The positive results using METX Engine Formula are as follows:
Numerous qualified engine tests were completed including small engines, 2-cycle, steam turbines, jet turbines, gasoline and the CRC L-38.  These tests have demonstrated the ability of METX Engine Formula to perform universally.  Further, these tests demonstrate that METX Engine Formula provides a protective effect that remains on the treated metal.  Four cylinder engines, after treatment with METX Engine Formula, have been stripped of valve covers, oil pans, oil-pumps and filters, with only the molecular thin film of METX Engine Formula, have successfully run without either oil or coolant, both on an engine stand and while completely submerged in water.  These tests have been run repeatedly and recorded before professional engineers.  The engines have been recorded to run in excess of 25 minutes while completely submerged under water.  The motors were later stripped and the components reviewed and re-weighed with little sign of wear.  

Additional tests: 

Test:  1
CRC L-38
Testing has been completed on a CRC L-38 Engine Stand ASTM D-5119-90 (American Society for Testing and Materials).  This rigorous test was conducted at prestigious Testing Centre in the US.

It is one of the largest independent automotive testing organizations in the world, providing testing to the automotive manufacturers and petrochemical industry since 1953. Their customers are worldwide, and include Shell Oil, Exxon-Mobil Oil, Chevron, Castrol, Pennzoil, Petro-Canada etc., along with automotive OEM’s, heavy-duty engine OEM, OEM suppliers and fuel and lubricant companies.  This firm was designated by the United States Petroleum Task force to regulate and control of the quality and acceptance of regulated additives. 

This firm was contracted to test the METX Engine Formula when combined with an off the shelf motor oil.  The reference oil used in the test was rated as a licensed API (American Petroleum Institute) spec motor oil,   The test is a gruelling 40 hours of severe running conditions plus 13 hours of run up and run down time.  The engine is run under full load at an RPM (revolutions per minute) of 3150 using an external oil heater to reach extreme oil temperatures of 290 degrees Fahrenheit (143.3 degrees Celsius) with fuel to run abnormally rich at 4.5 pounds per hour.  

The test is designed to break the down the oil, causing premature wear to the piston rod bearings, while have an adverse effect on the viscosity of the engine oil.  The reduced viscosity of the oil can create excessive wear and increase the amount of sludge and varnish build-up.
The scoring is based on a reference oil test on a particular machine. The reference oil must have passed the test on one of the many test machines.  The maximum allowable bearing loss is 40 mg of copper for the piston rod bearing.  Sludge and varnish deposits are scored best out of 10 points, with 10 being perfect.  

The engine assigned for the METX Engine Formula test was rated as the most difficult on which to obtain a passing score.  The reference oil recorded a bearing weight loss of 27.7-mg. of copper. 


The oil with the METX Engine Formula recorded a bearing weight loss of only 9.0 mg.  The engineer overseeing the test commented that it was one of, if not the best, test he has seen in over 12 years of service with Perkin Elmer. Further the results of viscosity, sludge and varnish tests were nearly perfect.  Out of a total of 60 possible points, the test with METX Engine Formula scored 58.30 and 58.80 respectively in varnish and sludge.  (The results exceeded all expectations.)  

Test 2
Oil Analysis:
                                
NEW
10 Hour
20 Hour
30 Hour
40 Hour
Acid Number                
2.00
2.90
3.50
3.80
4.00
Viscosity cSt 40°C    
102.90
101.90
101.60
101.50
102.10
Viscosity cSt 100°C    
14.13
13.89
13.82
13.79
13.84
Viscosity Increase





       CSt40°C                  
-4.37




Viscosity Increase





        CSt 100°C              
-8.35





Test:  3
Primary Parameter of Engine Deviations:
Tests were conducted on the various engine components at the completion of the test to evaluate any changes the test oil with the added METX Engine Formula may have had on the engine.  ASTM and the ACC (American Chemical Council) for the API (American Petroleum Industry) allow permitted deviation before a failure is recorded. 
                                                                       

Permitted
Calculated
Percentage
Deviation
Deviation
Engine Oil Gallery Temp
2.5
0.0
0
Engine Coolant Outlet Temp
2.5
0.0
0
Engine Coolant Delta Temp
2.5
0.0
0
Fuel Flow
2.5
0.0
0
Crankcase Off-Gas Std FT (3) h
2.5
0.0
0
Oil Press, PSI
2.5
0.0
0
Engine Speed, RPM
5.0
0.0
0
AFR
5.0
0.0
0
Exhaust, Hg
5.0
0.0
0

Note: These results of zero deviation exceeded all expectations.

Test: 4
Seta-Shell Four Ball Extreme Pressure Test (ASTM D-2783-82):
In this test, three steel test balls are locked in a holding cup while a fourth ball is fixed in a rotating chuck.  Lubricant is applied to the container holding the fixed and rotating bearings. 
Pressure is loaded on the force arm and the electric motor is started (to rotate the fourth bearing). 
The electric DC motor is set to run at a 1725 RPM for a specified time (such as 10.0 seconds) in this test.       
Wear Scar in Millimeters (4-ball method Scar Wear = mm)

Test Sample:   
Load K.G.F:
Time/Sec
A/Temp:
Scar Length:
Width:
METX  EF 
500
10
76° F
0.803
1.064
METX  EF         
780
10
76° F
1.043
1.337






Texaco™ 10W30    
500
10
76° F
2.94
2.44
Plus 10%  EF         
780
10
76° F
2.16
2.02
     





Esso™   10W30       
500
10
76° F 
2.91
2.51
Plus 10% EF            
780
10
76° F 
2.21
2.16
     





Motor Master™ 30   
500
10.0
76° F 
5
3.857
Plus 10% EF             
780
10.0
76° F 
2.074
1.951
     





Hydraulic AW46™ 
500
10.0
76° F 
2.9
2.32
Plus 10% EF              
780
10.0
76° F 
1.24
1.22
Notes:
• K.G.F. = Kilogram Force
• Weld or Failure = Score of 4.00 mm or greater
• EF = METX Engine Formula  

Test: 5
Analytical Report:
METX Engine Formula was tested with the analytical results posted below: 

ASTM Test No:
ASTM D-92
Flash Point
342°F/172.2° C
ASTM D-1298
Specific Gravity           
1.036
ASTM D-4739
Total Base No Mg KOH/g            
7.5
ASTM D-130
Copper Corrosion      1A
No Corrosion
ASTM D-97
Pour Point                   
-40° F/-40° C
ASTM D-445
Kinetic  Viscosity cSt 42.2        
40° C
ASTM D-445
Kinetic Viscosity cSt 8.8            
100° C
ASTM D-482
Ash Content
0.277


Test:  6
Metal Analysis: ASTM D-5185
A sample of METX Engine Formula was subjected to a metal analysis with the results posted below.

Aluminium                
None Detected
Barium                      
None Detected
Copper                      
None Detected
Chromium                 
None Detected
Iron                           
None Detected
Lead                          
None Detected
Molybdenum             
None Detected
Nickel                       
None Detected
Zinc                          
None Detected 
Silver                        
None Detected
Tin                            
None Detected
Vanadium                 
None Detected   
Test:  7
Block on Ring Test: (ASTM D-2981)
Block on Ring Machine: Ring O.D. is 40mm (1.57”).  
This test is normally performed at 800 RPM (329 FPM).  For the METX EF test, it was performed at 1725 RPM (699FPM), which is the maximum speed.  There was no cooling pump being run for the METX EF test.  The test oil specimen flows at 50ml/min (.013209 GPM or 3.05127 Cu. In. / Min.).  Standard Timken roller bearings were used with outer race of ANSI 52100 steel.  Mating blocks may be white metal, bronze on steel C 0.9, MN 1.2, Cr 0.5, W 0.5, V 0.1 (2510 AFNOR 90 MCW5 Case Hardened. To 58HRC).  Load on different blocks: steel/steel = 1075 RPM, bronze/steel = 358 RPM, white metal/Steel = 179 RPM. 

Test Routine:
The speed is first adjusted and then the load is steadily increased to the maximum permitted within a period of 5 minutes.  Each test was then run for ½ hour.  Recordings were made for maximum friction force and minimum friction force after run-in period. A stable curve was recorded at the end of test and maximum temperature was also recorded. 

After completion of over 80 tests, SEM (Scanning Electron Microscope) studies, for material reference and wear track studies showed the following:  

Friction Reduction:

10% Addition of METX EF 
Mineral Base Oil plus 10 % EF                   -10.6 %                  
Synthetic Base Oil plus 10% EF                 -10.6 % 

15% Addition of METX EF
Mineral Base Oil plus 15% EF                    -14.9%
Synthetic Base Oil plus 15% EF                 -48.9%  

Temperature Reduction:

10 % Addition of METX EF:  
Mineral Base Oil plus 10% EF                    -26.5%
Synthetic Base Oil plus 10% EF                 -17.0% 

15% Addition of METX EF:
Mineral Base Oil plus 15% EF                    -36.0%
Synthetic Base Oil plus 15% EF                 -38.7% 

Wear Reduction:

10% Addition of METX EF
Mineral Base Oil plus 10% EF                   -60.6%
Synthetic Base Oil plus 10% EF                 -40.3% 

15% Addition of METX EF
Mineral Base Oil plus 15% EF                   -78.8%
Synthetic Base Oil plus 15% EF                 -50.7%  


Test:  8
Engine Stand Testing 
A brand new NASCAR™ engine was provided for testing on a dynamometer.  The engine was run in on Kendall Racing Oil™ and numerous pulls were performed.  METX EF was then added to the Kendall Racing Oil ™ at a 10% ratio (20 parts oil to 2 parts METX EF).  The test is posted as below.

Dynamometer Test on 358 Cu. In. GM® Engine (5.8 Litre)
- The NASCAR™® Engine was set up and run in to full operating temperature at speeds to 6900 RPM.
- After multiple runs with Kendall Racing 20W50 Racing Oil ™, the maximum results were recorded in both horsepower and torque.  

- METX Engine Formula was then added at a 10% ratio and the tests repeated with maximum results recorded.

Results:
- STPPwr-Chp Kendall®                                                            Maximum Horsepower = 494
- STPPwr-Chp with 10% METX EF added to Kendall®,         Horsepower = 508
- STPTrq-Clb-ft Kendall®                                                          Maximum Torque = 399

- STPTrq-Clb-ft Kendall® plus 10% METX EF added,           Torque = 411

Test:  9
Copper Corrosion Test:   ASTM D-130

The tests were carried out on polished copper blanks that were submerged, for 3 hours at at100 degrees C, in oil treated with 15% of METX Engine Formula and a number of its blended by-products. The blanks were then withdrawn, washed in Stoddard’s solvent and the colors of the blanks were compared with a standard chart.  The results of the tests consistently revealed 1-A, meaning “No Corrosion”. 


Test:   10
Rheological Evaluation:

Rheological evaluation was performed on the METX Engine Formula when blended with various conventional motor oils.  The test is to examine the effect that METX EF can have when blended with a host oil.

The samples oils tested with 10% and 15% addition of METX EF displayed Newtonian behavior (the desired results) at all temperatures tested.  The treated oils displayed a substantial improvement in minimizing thermal degradation with the addition of METX EF.  Using standard regression techniques, the variations of oil viscosities with each temperature was found to follow the Arrhenius model, AE/RT (n = Ae) (excellent result).

Further tests conducted on METX EF include, but are not limited to:     
     
Engine Tests:  All Tests Were Passed with Exceptional Results        
 
Sequence VI B Fuel Economy Test with Energy Conserving Oil     
    
Sequence VI B SJ Fuel Economy Test with Energy Conserving Oil    
     
Sequence VIII Bearing Corrosion and Shear Stability with Energy Conserving Oil    



Test 11
(A)   METX Pro Lube Penetrant Tests, Information and Results:
  
             
ASTM D 2782-83: the Standard Test Method for Extreme Pressure Properties        
ASTM D 4172: the Standard Test Method for Wear Test Properties
        

Note: The 4-ball wear or weld tester consists of 4 balls arranged in the form of an equilateral tetrahedron.  The three lower balls are held immovable in a clamp (chuck) to form a cradle in which the fourth ball is caused to rotate around a vertical axis under prescribed conditions of load, speed and temperature.  Ten ml of the lubricant are placed with the ball pot and, after the test is completed, the wear scar is measured, length and width, on each of the three balls.   The spinning ball is not measured.  Pressure exerted upon the balls is measured in KgF. (Kilogram Force)             
ASTM D 2782-83 Extreme Pressure Test        Speed: 800 RPM                                                     
Prod
Test No
Load
Time-sec:  
Temp
Scar mm 
Scar mm
Amb
Width
Length
METX EF
1
150 KgF
10
76° F
0.549
1.28
2
150 KgF
10.4
76° F
0.583
1.36
3
150 KgF
10.2
76° F
0.557
1.3
Result
Ave
0.563
1.31
Ave
0.964
Leading cleaner Lubricant
          
1
150 KgF
-10
76° F  
5.0 Weld
5.0 Weld
2
150 KgF
-10
76° F  
5.0 Weld      
5.0 Weld
3
150 KgF
-10
76° F  
5.0 Weld
5.0 Weld
Result
Ave
5.0 Weld


Note: With Leading Cleaner, Lubricant, there was a large amount of metal deformation taken off the spinning ball in the chuck and deposited on the three stationary or locked balls.  According to the ASTM D2782 test, with stationary balls, a scar size of 4 mm or greater is considered a weld, or total failure.             

                      

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